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Spectral Data   Additional Data   Download  
Type: 1H 500.0
Atom
No. ⇓
Mult.(coupling const.)
Meas.
Shift
1-H m;m 1.07, 0.85
2-H m;m 1.67, 1.41
3-H m;m 1.34, 1.17
5-H m 0.84
7-H m;m 1.57, 1.38
8-H dt (12.5);m (3.2) 1.77, 1.05
10-H dd 0.99 (H 30)
11-H m 1.63 (H 29)
13-H dt (12.5);m (3.2) 2.02, 1.65
14-H m;m 1.71, 1.32
15-H d;d 2.56
19-H br s 6.55
21-H dd (8.4) 6.56
22-H d (8.4) 6.62
23-H
24-H s;s;s 1.16
25-H s;s;s 0.88
26-H m;m;m 0.85
27-H s;s;s 0.86
28-H s;s;s 0.82





Spectral Data   Additional Data   Download  
13C Spectrum
60006192 Rating: 9 (9: 9: nmrshiftdb2 quality check: accept/reliability: good (admin))
Type13C
Measurement conditions
Temperature [K]298
SolventChloroform-D1 (CDCl3)
Field Strength [MHz]125.0
Assignment Method1H, H,H-COSY, H,H-NOESY, H,C-HMQC, H,C-HMBC, DEPTQ, 1H, 13C, 1H, H,H-COSY
Literature Yasuji Yamada; Rob W. M. van Soest; Ayako Hoshino; Akinori Shintani; Hidemichi Mitome; Hiroaki Miyaoka: Journal of Natural Products, in: New Strongylophorines from the Okinawan Marine SpongePetrosia , vol. 66/2003, pp. 1600 - 1605 (DOI: 10.1021/np030312q).
Additional commentsd3-20373
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Spectrum categoriesocmainz inhouse-2




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