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Details
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This molecule without stereoconfiguration:
ChiuZ/Chloroform-D1 (CDCl3)
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Type: 13C 150.0 Double click to get resizeable window!
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Atom
No.
⇓
|
Mult.(coupling const.) |
Meas. Shift
|
1
|
S |
151.2 |
2
|
S |
141.7 |
3
|
S |
153.6 |
4
|
D |
107.4 |
5
|
T |
29.9 |
6
|
T |
36.5 |
7
|
D |
52.7 |
8
|
D |
130.5 |
9
|
S |
179.5 |
10
|
S |
164.1 |
11
|
D |
112.9 |
12
|
D |
135.6 |
13
|
Q |
61.6 |
14
|
Q |
61.4 |
15
|
Q |
56.2 |
16
|
Q |
22.8 |
16
|
Q |
56.5 |
17
|
S |
170.1 |
4a
|
S |
134.3 |
7a
|
S |
152.6 |
12a
|
S |
137.0 |
12b
|
S |
125.6 |
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Type: 1H 600.0 Double click to get resizeable window!
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Atom
No.
⇓
|
Mult.(coupling const.) |
Meas. Shift
|
18-H
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|
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4-H
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6.550 |
5-H
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2.390, 2.520 |
6-H
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1.956, 2.350 |
7-H
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4.660 |
8-H
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7.630 |
11-H
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(10.9) |
6.900 |
12-H
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(10.9) |
7.356 |
13-H
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3.660 |
14-H
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3.940 |
15-H
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3.910 |
16-H
|
|
1.970 |
16-H
|
|
4.010 |
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Type: H,C-HSQC 600.0 Double click to get resizeable window!
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Axis: 1 (H) |
Axis: 2 (C) |
Atom
|
Shift
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Shift
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6
|
1.95 |
36.5 |
16
|
1.97 |
22.8 |
6
|
2.35 |
36.5 |
5
|
2.39 |
29.9 |
5
|
2.52 |
29.9 |
13
|
3.66 |
61.6 |
15
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3.91 |
56.2 |
14
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3.94 |
61.4 |
16
|
4.01 |
56.5 |
7
|
4.65 |
52.7 |
4
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6.53 |
107.4 |
11
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6.9 |
112.9 |
12
|
7.36 |
135.6 |
8
|
7.63 |
130.5 |
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Type: H,C-HMBC 600.0 Double click to get resizeable window!
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Axis: 1 (H) |
Axis: 2 (C) |
Atom
|
Shift
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Atom
|
Shift
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6
|
1.95 |
5
|
29.9 |
6
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1.95 |
7
|
52.7 |
6
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1.95 |
4a
|
134.3 |
16
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1.97 |
17
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170.1 |
6
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2.35 |
5
|
29.9 |
6
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2.35 |
7
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52.7 |
6
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2.35 |
7a
|
152.6 |
5
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2.39 |
4a
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134.3 |
5
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2.39 |
12b
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125.6 |
5
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2.39 |
4
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107.4 |
5
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2.39 |
6
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36.5 |
5
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2.52 |
6
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36.5 |
5
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2.52 |
7
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52.7 |
5
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2.52 |
4
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107.4 |
5
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2.52 |
12b
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125.6 |
5
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2.52 |
4a
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134.3 |
13
|
3.66 |
1
|
151.2 |
15
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3.91 |
3
|
153.6 |
14
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3.94 |
2
|
141.7 |
16
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4.01 |
10
|
164.1 |
16
|
4.01 |
11
|
112.9 |
7
|
4.65 |
7a
|
152.6 |
7
|
4.65 |
6
|
36.5 |
7
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4.65 |
8
|
130.5 |
7
|
4.65 |
12a
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137.0 |
7
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4.65 |
17
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170.1 |
4
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6.53 |
5
|
29.9 |
4
|
6.53 |
12b
|
125.6 |
4
|
6.53 |
2
|
141.7 |
4
|
6.53 |
1
|
151.2 |
4
|
6.53 |
3
|
153.6 |
4
|
6.53 |
4a
|
134.3 |
11
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6.9 |
12a
|
137.0 |
11
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6.9 |
10
|
164.1 |
11
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6.9 |
9
|
179.5 |
12
|
7.36 |
12b
|
125.6 |
12
|
7.36 |
12a
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137.0 |
12
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7.36 |
7a
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152.6 |
12
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7.36 |
10
|
164.1 |
8
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7.63 |
7
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52.7 |
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Axis: 1 (H) |
Axis: 2 (C) |
Atom
|
Shift
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Atom
|
Shift
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|
8
|
7.63 |
12a
|
137.0 |
8
|
7.63 |
7a
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152.6 |
8
|
7.63 |
10
|
164.1 |
8
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7.63 |
9
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179.5 |
18
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8.12 |
7
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52.7 |
18
|
8.12 |
17
|
170.1 |
18
|
8.12 |
6
|
36.5 |
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H,H-NOESY Spectrum | 60000197
Rating: 10 |
Type | H,H-NOESY |
Measurement conditions
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Temperature [K] | 298 |
Solvent | Chloroform-D1 (CDCl3) |
Field Strength [MHz] | 125.0 |
Literature |
Johannes Appun; Hans-Ullrich Siehl; Klaus-Peter Zeller; Katrin Steinke; Stefan Berger; Dieter Sicker: Colchicin, in: Chemie in unserer Zeit, vol. 48/2014, pp. 36 - 44 (DOI: 10.1002/ciuz.201400653)
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Additional comments | |
Additional information |
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Spectrum categories | ChiuZ |
Report incorrect data
Copy dataset link
DOI for this dataset: 10.18716/nmrshiftdb2/60000009/chiuz_cdcl3
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